中华人民共和国国家环境保护标准HJ963-2018固体废物有机磷类和拟除虫菊酯类等 47种农药的测定气相色谱-质谱法Solid waste —Determination of 47 organophosphorous and pyrethroidpesticides— Gas chromatography mass spectrometry（发布稿）本电子版为发布稿请以中国环境出版社出版的正式标准文本为准2018-07-29发布2019-01-01实施发布生态环境部 目次前言.................................................................................................................................................ii1适用范围.........................................................................................................................................12规范性引用文件.............................................................................................................................13方法原理.........................................................................................................................................14试剂和材料.....................................................................................................................................15仪器和设备.....................................................................................................................................26样品.................................................................................................................................................37分析步骤.........................................................................................................................................58结果计算与表示.............................................................................................................................89精密度和准确度...........................................................................................................................1010质量保证和质量控制.......................................................................................................